ojs2 has produced an error Message: WARNING: mkdir(): Permission denied In file: /var/www/html/ojs246_old/lib/pkp/classes/file/FileManager.inc.php At line: 306 Stacktrace: Server info: OS: Linux PHP Version: 5.6.33-0+deb8u1 Apache Version: Apache/2.4.10 (Debian) DB Driver: mysql DB server version: 5.7.27
ojs2 has produced an error Message: WARNING: assert(): Assertion failed In file: /var/www/html/ojs246_old/plugins/generic/usageStats/UsageStatsPlugin.inc.php At line: 308 Stacktrace: Server info: OS: Linux PHP Version: 5.6.33-0+deb8u1 Apache Version: Apache/2.4.10 (Debian) DB Driver: mysql DB server version: 5.7.27
The Ultrasonic Extraction Method for Determination of Sulfonamide | Navakhun | งดใช้ระบบ 3-31 กค 66 Burapha Science Journal

The Ultrasonic Extraction Method for Determination of Sulfonamide

Apinya Navakhun, On-u-ma Petplian, Anurak Chankaew

Abstract


The ultrasonic extraction method for determination of 5 sulfonamides residues in chicken was studied. The amount of sulfonamides was analyzed by high performance liquid chromatographic technique. The extraction parameters such as type of organic solvent, extraction time, volume of organic solvent and extraction temperature were carried out in order to increase the extraction efficiency. In extraction process, the synthetic chicken of 2.0 g was used. The optimum solvent was 5 mL of acetonitrile. The extraction time and extraction temperature were 30 min and 30 °C, respectively. Under the optimum conditions, detection limit and quantification limit were 0.03-0.06 and 0.20-0.40 mg/L, respectively. The linear was in range of 0.20-2.40 mg/L with R2 more than 0.9917. The %RSD and %recovery were 0.41-19.92 and 52.52-151.14%, respectively. The extraction efficiency of this method was more than 90%.


Full Text:

PDF

References


Thiele-Bruhn S. (2003) Pharmaceutical antibiotic compounds in soil—a review. Journal of Plant Nutrition and soil Science. 166, 145–67.

National Veterinary Research and Quarantine Service (NVRQS)(2005). Establishment of control system of antibiotics for livestocks. Korea Food and Drug Administration.

European Council Regulation 2377/90/EC (1990). A community procedure for the establishment of maximum

residue limits of veterinary medicinal products in foodstuffs of animal origin. 224.

Stoev, G., Michailova, A., (2000). Quantitative determination of sulfonamide residues in foods of animal origin by high-performance liquid chromatography with fluorescence detection. Journal of Chromatography A, 871, 37-42.

Förster, M., Laabs, V., Lamshöft, M., Pütz, T. and Amelung ,W. (2008). Analysis of aged sulfadiazine residues in soils using microwave extraction and liquid chromatographytandem mass spectrometry. Analytical and Bioanalytical Chemistry 391:1029–1038

Raich-Montiu, J., Beltrán, J. L., Prat, M. D, Granados, M. (2010). Studies on the extraction of sulfonamides from agricultural soils. Analytical and Bioanalytical Chemistry. 397, 807-814.

Andrzej, P., Jan, Z., and kamila M. (2005). Dispersive solid-phase extraction for the determination of sulfonamides in chicken muscle by liquid chromatography. Journal of Chromatography A. 1087, 259-264.

Hela, W., Brandtner, M., Widek, R., Schuh, R. (2003). Determination of sulfonamides in animal tissues using cation exchange reversed phase sorbent of sample cleanup and HPLC-DAD for detection. Food Chemsitry. 83, 601-608.

Chen, L., Zeng, Q., Wang, H., Su R., Xu, Y., Zhang, X., et al. (2009). On-line coupling of dynamic microwave assisted extraction to solid-phase extraction for the determination of sulfonamide anitibiotics in soil. Analytica Chimica Acta. 648, 200-206.

AOAC International. (1993). AOAC peer-verified method program: manual on policies and procedures. United States of America.


Refbacks

  • There are currently no refbacks.